ASTM A453 Grade 660 Class D (660D) is solution treated at 1650 ± 25 °F [900 ± 14 °C] for 2 h min or 1800 ± 25 °F [980 ± 14 °C] for 1 h min and liquid quenched, then aged at 1325 ± 25 °F [720 ± 14 °C] for 16 h and air cooled, with a second age at 1200 ± 25 °F [650 ± 14 °C] for 16 h if needed to reach the properties (A453/A453M-17 Table 4). Table 5 requires up to 2½ in. [63.5 mm]: 130 ksi [895 MPa] tensile and 105 ksi [725 MPa] yield; over 2½ in. [63.5 mm]: 120 ksi [825 MPa] tensile and 95 ksi [655 MPa] yield; 15 % elongation, 18 % reduction of area and 248 to 321 HB (24 to 35 HRC) in both size ranges; A453/A453M-17 added the separate large-size limits. Class D does not require a stress-rupture test and is stamped NR in addition to the other required markings (8.2.1, 9.1). Unlike Class A, B and C, Class D has a 105 ksi [725 MPa] minimum yield up to 2½ in., a 321 Brinell maximum instead of 341 (approximately 35 HRC instead of 37 HRC), and no stress-rupture test. API 6A (21st edition) 8.2.3.2 sets the same 35 HRC maximum and 725 MPa / 655 MPa yield split for 660D bolting, and ISO 15156-3 (NACE MR0175) also limits UNS S66286 to 35 HRC. API 20F covers Grade 660 Class D for BSL-2 and BSL-3 bolting. NORSOK M-630:2020 MDS S39 Rev. 1 covers A453 Gr. 660 Class D studs, bolts and nuts with Charpy V testing at -101 °C: 27 J average, 20 J single, 0.38 mm lateral expansion. ASTM A453 Grade 660 Class D bolting to MDS S39 is manufactured at TorqBolt.
API 6A (21st edition) 8.2.3.6 states that ASTM A453/A453M Grade 660D solution-treated and age-hardened bolting should not be used on pressure containing and high load bearing connectors in the following situations :
wet/dry offshore and coastal applications in the presence of salt air;
where it is routine to clean/wash equipment with untreated/raw seawater.
NOTE 1 - Environmentally assisted cracking, such as stress corrosion cracking (SCC), may result from the presence or accumulation of Chlorides from deposited salt on highly stressed austenitic stainless steel bolting, such as Grade 660D .
NOTE 2 - API 6ACRA addresses alternative, higher-strength CRA materials suitable for sour exposure .
Annealing & Ageing Cycles
Grade Symbol
Class
Solution Treatment
Hardening Treatment
ASTM A453/A453M Grade 660
D
1650 ± 25 °F [900 ± 14 °C], hold 2 h min, and liquid quench or 1800 ± 25 °F [980 ± 14 °C], hold 1 h min, and liquid quench
1325 ± 25 °F [720 ± 14 °C], hold 16 h, air cool If necessary to achieve properties, second age: 1200 ± 25 °F [650 ± 14 °C] hold 16 h, air cool
(A) Times refer to the minimum time material is required to be at temperature.